Semester – III

INDUSTRIAL ECONOMICS (HUM201) 

Unit –I

Introduction to Economics:

Introduction to economics, its Importance, Principals, Approaches, and use of study, Engineering and economics, Economic problems, economic good and wealth, Demand and supply, Competition, Monopoly, theory of firm, Money and its function, theory of money and choice, the bank and its functions, employment and income, Gross National Product, Net National Product Consumption, Savings and investment.

Unit –II

Features of Indian Economy-I:

Broad features of Indian Economy, Natural resources and economic development, Infrastructure in the Indian Economy, Agriculture development, Green revolution, Population, Population theories, Unemployment, Poverty, and Balance Regional Development. Economic Growth and Economic Development, Indian Industries, Industrial Policy, Industrialization in India, role, plan and pattern of Industrialization, Public vs Private Sectors, Economic reforms in India, India’s Five Year Plans.

Unit– III

Features of Indian Economy-II:

The indigenous and modern banking system in India, Reserve Bank of India, Monetary and Fiscal Policies, Financial Institutions and SEBI, Free trade and protection, India’s Foreign Trade and WTO, Balance of Payments, Indian Currency System and Foreign exchange, Foreign Capital Investment, Foreign Aid, and FEMA.

Unit –IV

Introduction to Business Organization-I:

Concept, nature and scope of business, business and its environment, Profit maximization vs social responsibility of business, business ethics, business enterprise, entrepreneurship, Promoters, types and functions, stages in company formation, concept of business growth, rationale and types of growth strategies, joint venture-definition, scope, role and problems of small business, concepts and features of public enterprise, multinationals.

Unit– V

Introduction to Business Organization-II:

Time value for money, Simple and compound interest, annuity, Depreciation, definitions, characteristics, Life and Salvage value, Method of providing for depreciation, relationship between depreciation, repairs, renewals, Depletion cost, Replacement, Amortization, and Present worth.

Suggested Text books and references:

1. Indian Economy --Dutt & Sundaram

2. Engineering Economics –Tarachand

3. A Text Book of Economic Theory --Stonier & Hague

4. Business Organization --Shukla 

Introductions to Chemical Engineering (CH-201)

Unit I  

Historical overview of Chemical Engineering: Concepts of unit operations and unit processes, and recent developments.

Unit II 

Fuels –Solid, liquid  & Gaseous fuels.  

Unit III

Chemical Kinetics Constant Rate constant order and molecularity of a reaction, zero, 1^st, 2^nd, and 3^rd order reactions. Kinetics of opposing reactions, methods of determination of order of reactions. Reaction rate theories, Arrhenius Parameters, Catalysis (including enzyme catalysis), effect of catalysis on reaction rate. 

Unit IV

Introduction to Heat Transfer, Conduction, Convection, Radiation, Flow Arrangement in Heat Exchangers, Variation of Fluid Temperature in Heat Exchangers, Heat Transfer Equipment, Evaporation, Problems. 

Unit V

Introduction to Mass Transfer, crystallization, distillation, evaporation absorption.

Texts/References

1.   R. M. Felder and R.W. Rousseau, Elementary Principles of Chemical Processes, 3rd ed., John Wiley, New York,

2.   Enderson & Belzil Introduction to Chemical Engineering            

3.   Bezer & Banchoro, Introduction to Chemical Engineering

4.   Salil. K Ghosal, Shyamal K Sanyal, Siddhratha Datta “Introduction to Chemical Engineering, Tata McGraw Hill, New Delhi.

Instrumentation & Measurement (CH-202) 

Unit-I        Measurement and error. Accuracy and precision, sensitivity, resolution, Types and sources of errors. PMMC, Analog meters, Electronic Voltmeters and Ammeters. (C and DC) Electronic millimeters, AC probes, CROs, VIVM.

Unit-II       Measurement of inductance and Q of the coil. Maxwell’s Bridge, Wien’sbridge, Schering bridge, wagner’s earth, vector impedance meter transducers (LVDT). Photoelectric transducers.

Unit-III     Signal generator, function generator. Function generator, sweep frequency generator. Pulse and square wave generator, Heterodyne, Frequency meter frequency counter. Measurement errors.

Unit-IV      Digital instruments: Advantage of digital instruments, over analog instruments, D-A, A-D conversion. Digital voltmeter, Ramp type DVM, Integrating DVM, Successive approximation DVM Displays (LED. LCD and seven segment etc.)

Unit-V       Temperature & Pressure measurements, Thermocouples. Photosensitive device, Pressure measuring. Wave Analyzers, Spectrum Analyzer, Instruments used in computer controlled instrumentation, RS232C and IIEE488, GPIB electrical interface, Interfacing transducers to electronic control pressure gauges.

Reference Books: 

1.     Albert D. Cooper – Modem Electric Instrumentation – PHI 

2.     A.K. Maini-Microwave & RADARS – Khanna Publisher.

Chemical PROCESS CALCULATIONS (CH-203)

Unit I

STOICHIOMETRY: Introduction- Units and Dimensions - stochiometric principles-composition relations, density and specific gravity.

Unit II

IDEAL GASES AND VAPOR PRESSURE: Behaviors of Ideal gases -kinetic theory of gases - application of ideal gas law- gaseous mixtures - volume changes with change in composition. Vapor pressure- effect of Temperature on vapor pressure-vapor pressure plots-vapor pressure of immiscible liquids-solutions.

Unit III

HUMIDITY AND SOLUBILITY: Humidity - saturation - vaporization - condensation - wet and dry bulb thermometry Solubility and Crystallization-Dissolution -solubility of gases.

Unit IV

MATERIAL BALANCE:  Material Balance - Processes involving chemical reaction - Combustion of coal, fuel gases and sulphur-Recycling operations - bypassing streams - Degree of conversion -excess reactant - limiting reactant

Unit V

ENERGY BALANCE: Thermo chemistry - Hess's law of summation - heat of formation, reaction, combustion and mixing - mean specific heat -Theoretical flame Temperature.

TEXTBOOKS:

1.      O.A.Hougen, K. M. Watson and R. A. Ragatz, "Chemical Process Principles", Vol-I,CBS Publishers and Distributors, New Delhi, 1995.

2.      D. Himmelblau, '"Basic Principles and Calculations in Chemical Engineering", 5^th Edn.,Prentice Hall of India Ltd.,N.Delhi,1994.

REFERENCES:

1.      B.I.Bhatt and S.M.Vora, "Stoichiometry", Tata McGraw Hill Publishers Ltd., New Delhi, 1996.

2.      V.Venkataramani and N.Anantharaman,"Process Calculations",Prentice Hall of India Ltd.,N.Delhi,2003.

Fluid Mechanics (CH-204)

Unit-I        Introduction : Properties of fluid, forces on fluid, stresses, the concept of constitution relations, fluid statics, Normal forces in fluid, pressure Measurement, forces on submerged, forces on submerged bodies, buoyancy, stability.

Unit-II       Classification of Fluids : Newtonian and Non-Newtonian fluid, Viscosity measurement, Equations of Continuity & Equation of Motion. Navier stokes equation, concept of Reynolds number and friction factor : friction factor for rough and smooth pipes, loss of head due to friction in pipes and fittings.

Unit-III     Boundary layer theory, Bernoulii’s equation, fluid machinery pump fans blowers, compressor & vacuum pumps. Power and head requirement for pumps.

Unit-IV      Flow of incompressible fluid in conduits and thin layers, flow past immersed bodies. Dimensional analysis, Buckingham p - theorem, dimensionless numbers and their significances, similitude criteria.

Unit-V       Measurement of flow: Fluid flow Measurement pitot tube, orifice meter, venture meter, Rota meter weirs and notches.

Reference Books:

1.     W.L. McCabe & I.C. Smith – UNIT OPERATIONS IN CHEMICAL ENGG. – McGraw Hill & Kogakusha 1976. 

2.     J.M. Coulson & J.F. Richardson – CHEMICAL ENGINEERING – Vol I & II 

3.     B.S. Maney, zel (SI) Van Nostand & Reinhold – MECHANICS OF FLUID – ELBS, 1970 

4.     I. Grannet – FLUID MECHANICS FOR ENGG. AND TECHNOLOGY – Prentice Hall, 1971 

5.     Maurice G. Larian – FUNDAMENTALS OF CHEMICAL ENGG. OPERATION – Constable and Company Ltd. Landon. 

6.     S.K. Gupta – MOMENTUM TRANSFER-Newage Publication.

Computer Programming – II (CH-205)  

Unit I

Objects And Classes: Concepts in object-oriented programming, classes and objects, C++ programming basics, object-oriented analysis, object-oriented design methods.

Working With Classes: Operators and Friends: Operator overloading, Friend functions and operators. Arrays, Pointers and References.

Unit II

Class Inheritance: Derived classes, the protected access specifier, derived class constructors, overriding member functions, Class hierarchies, Public and Private inheritance, multiple inheritances.

Unit III

Polymorphism: Virtual functions, Abstract base classes and pure virtual functions.

Unit IV

Files And Streams: Introduction to object-oriented database - case studies.

TEXT BOOK: 

1.    Robert Lafore, "Object Oriented Programming Turbo C++", Gaogotia Pub. 1992. 

REFERENCES : 

1. Neill Graham, "Leaning C++", McGraw Hill Inc. Intl. Edn.,1991. 

2.     Roger S. Pressman, "Software Eng.," A Practitioner’s Approach, McGraw Hill 3^rd Edn ., 1992. 

Technical Analysis Lab (CH-241)

List of Experiments:

1.    Application of pH meter to find acidity and alkalinity of a solution.

2.    Proximate analysis of coal sample         

3.     To determine the moisture content of coal sample. 

4.     To determine the ash content of coal sample. 

5.     To determine the turbidity in wastewater sample by Nephlometer, chloride in wastewater sample. 

6.     Determination of pH, temperature and conductivity of given sample by electrode method.

7.     Determination of the strength of unknown strong acid by titrating it against weak base by conductometric method. 

8.     Determination of pH of mixture of CH₃COOH and CH₃COONa and the dissociation constant of the acid. 

9.     Chemical analysis of cement. 

10. Analysis of fertilizer.

Fluid Mechanics Lab (CH-242)

List of Experiment:

1.     To determine the local velocity pressure with the help of pilot tube. 

2.     To find out the terminal velocity of a spherical body in water. 

3.     To determine the viscosity of a given viscous liquid by capillary tube flow method. 

4.     To find the pressure drop in a packed bed. 

5.     To study the flow behaviour of a non-Newtonian fluid and to determine to flow constants.

6.     To determine to power-number-Reynolds number curve for an agitated vessel. 

7.     To differentiate between laminar and turbulent flow using Reynolds experiment. 

8.     To study the characteristics of an air compressor. 

9.     To study the characteristics of a centrifugal pump. 

10. To study the flow of a fluid in a pipeline and to prepare the friction factor – Re plot. 

11. To determine velocity through orifice meter, venture meter. 

12. To prepare the calibration curve for an orifice meter and Rota meter.

13. To Calculate to prepare the calibration curve for venturimeter.

Semester – IV

NUMERICALTECHNIQUES (MTH-251) 

Unit I

NON-LINEAR EQUATIONS: Solving non linear equations-Regula Falsi method-Newton's method-order of convergence-Graeffe's method and Bairstow's methodincluding the case of pairs of complex roots-Newton's method for f(x,y)=0,g(x,y)=0.

Unit II

LINEAR SYSTEMS: Solution of linear equations-Gaussian elimination,Gauss Jordan and Crout's methods-Finding the inverse of a matrix using elementary row transformations-Gauss Seidel and Jacobi iterative methods-Power method to find dominant eigen value and eigen vector.

Unit III

INTERPOLATION AND CURVE FITTING: Newton's forward and backward interpolation-Lagrange's interpolation-Newton's divided difference method-cubic spline interpolation-natural splines-choosing appropriate curve and fitting to data-curve fitting-Method of least Squares-regression equations.

Unit IV

NUMERICAL SOLUTION OF ODE (Ordinary Differential Equation):Euler's method-Euler's modified method-Taylor's method - Runge-Kutta method of second and fourth order-Simultaneous equations and higher order equations by Taylor's method and Runge-Kutta method-Multistep method-Milne's and Adams' predictor-corrector methods.

Unit V

NUMERICAL SOLUTION OF PDE (Partial Differential Equation):Boundary value problems - finite difference methods - second order linear PDEs - solution of Laplace and Poisson equation by Liebmann's method - solution of one Dimensional heat flow and wave equations.

TEXT BOOKS:

1.         M. K. Venkataraman, "Numerical Methods in Science and Engineering" NPC 2^nd Edn.,(For Unit I)1986.

2.         M.K.Jain, SRK lyengar and R.K.Jain, "Numerical Methods for Scientific and Engineering Computation", Wiley Eastern, 1992.

 REFERENCE:

1.         C.F. Gerald, "Applied Numerical Analysis", 2^nd Edn., Addison Wesley Publishing Company (For Unit I) 1978, 4^th Edn., 1989.

CHEMICAL ENGINEERING THERMODYNAMICS (CH-251) 

Unit I

FUNDAMENTALS OF THERMODYNAMICS: Laws of thermodynamics as applied to open and closed system - reversible and irreversible processes - state and point function - Absolute entropy - Thermodynamic property changes for ideal gas.

Unit II

PVT RELATIONS: PVT relationships for gases and liquids - equations of state - Z charts - gas mixtures. Compression - expansion. Refrigeration: Principles and application.

Unit III

THERMODYNAMIC RELATIONS: Thermodynamic relations - Maxwell's relations - Jacobian algebra - estimation of thermodynamic properties.

Unit IV

PHASE EQUILIBRIA: Phase equilibria - pure component and mixtures - Latent heat correlation - van Laar, Margules equations - Gibbs' - Duhem equation - consistency tests - partially miscible and immiscible systems - Azeotropes - retrograde condensation - thermodynamic diagrams.

Unit V

CHEMICAL EQUILIBRIA: Chemical equilibria - heat effects, industrial reactions - Free energy calculations - Homogeneous and heterogeneous reactions - Industrial reactions like NH3 synthesis, SO3 production etc.

TEXTBOOKS:

1.      J. M. Smith and Van Ness, "Introduction to Engineering Thermodynamics", McGraw Hill, New York, 1994.

2.      V.C. Rao – Chemical Engg Themodynamics.

 REFERENCE:

1. B.F. Dodge, "Chemical Engineering Thermodynamics", McGraw Hill, New York, 1971.  

Mechanical Operations (CH-252)

Unit I

CHARACTERISTICS OF PARTICULATE SOLIDS AND SIZE REDUCTION & SCREENING: Properties and characterization of particulate solids, analysis and technical methods for size and surface area distribution of powder; Introduction to size reduction equipment, energy and power requirement in milling operations, computer simulation techniques for mill performance. Mechanical classifiers: Screening equipment, capacity and effectiveness.

Unit II

FILTRATION: Filtration equipment, filtration media and filter aids, principles of filtration and clarification, estimation of filtration parameters for compressible and incompressible cakes and calculations, centrifugal filtration equipment and principles of operation.

Unit III

SETTLING AND SEDIMENTATION:  Separation based on the motion of particles through fluids, gravity settling processes, Sedimentation, Kynch theory of sedimentation, equipment for sedimentation thickness, rate of sedimentation and sedimentation zones in continuous thickeners, design of thickeners and clarifiers, principles of centrifugal sedimentation and characteristics and sedimenting centrifuges.

Unit IV

AGITATION AND MIXING OF LIQUIDS: Introduction to agitation and mixing of liquids, agitation equipment, Axial and radial flow impellers and flow patterns in agitated vessels ,prevention of swirling, power consumption in agitated vessels, Blending and mixing, dispersion operations, mixing of solids and pastes and types of mixers.

Unit V

STORAGE AND CONVEYING OF SOLIDS:Introduction to storage and conveying of solids, bins, hoppers and silos, flow out of bins, design consideration of bins, loading and unloading of solids. Bucket elevators, apron conveyors. Belt conveyors: types of belt conveyors, selection considerations.

TEXTBOOKS:

1.         McCabe and J.C.Smith,"Unit Operation of Chemical Engineering", 5^th Edn., McGraw Hill, New York, 1993.

2.         J.M.Coulson and J.F .Richardson, "Chemical Engineering", Vol.II, 4^th Edn., Butterworth - Heinemann, 1991.

3.         L.N. Foust

4.         Brown

REFERENCE :

1.         Raymond A. Kulweic, "Materials Handling Handbook",2^nd Edn, Wiley-Interscience Publications, 1985.

2.         Badger and Banchero, "Introduction to Chemical Engineering", 1^st Edn., McGraw Hill, NewYork, 1954.

Material Science & Technology (CH-253)

Unit-I        Mechanical, Thermal &Electrical properties of Materials and their measurement.

Unit-II       Atomic structure, Inter atomic attraction, Molecular structure, crystallanity, Solid solutions, crystal imperfections, Electronic structure and Electromagnetic properties/

Unit-III     Single phase metal deformation, Failure of Metals, Theories of alloying, phase relationship, ironcarbon diagram, Nomenclature of steels, utilization of cast iron, mild steel, stainless steel, lead and graphite in Chemical Engg. System.

Unit-IV      Theories of Corrosion and corrosion – control, stability of materials in service: Chemical, Thermal and Radiolytic stability.

Unit-V       Composite materials; Semiconductors, Superconductor, surface Modifications using linings of plastics, rubber, glass, ceramics etc., Nano-materials.

  Reference Books:

1.     VAMBLACK, MATERIAL SCIENCE

2.     WOOLEF,: VOL. 1,2,3,4. 

3.     Robert H. Perry & Don W. Green-PERRYS CHEMICAL Engineering H AND BOOK – VII Ed. – McGraw Hill. 

4.     O.P. Khanna – MATERIAL SCIENCE & METALLURGY – Dhanpat Rai Publication. 

5.     S.K. Hajra Choudhury – MATERILS SCIENCE & PROCESSES – Indian Book Distributing Co.

CHEMICAL PROCESS TECHNOLOGY-I (CH 254) 

Unit-I. ALKALIES:

Chlor-alkali Industries: Manufacture of Soda ash, Manufacture of caustic soda and chlorine - common salt.  

Unit-II. ACIDS: 

Sulphur and Sulphuric acid: Mining of sulphur and manufacture of sulphuric acid. Manufacture of hydrochloric acid .

Unit-III. CEMENT AND GLASS

Cement: Types and Manufacture of Portland cement. Glass: Manufacture of glasses and special glasses. Ceramics: Refractories.

Unit-IV. INDUSTRIAL GASES & PAINTS:

Industrial Gases: Carbon dioxide, Nitrogen, Hydrogen, Oxygen and Acetylene - Manufacture of paints - Pigments.

Unit-V. FERTILISERS:

Nitrogen Fertilizers: Synthetic ammonia, nitric acid, Urea, Ammonium Chloride, CAN, Ammonium Sulphate - Phosphorous Fertilizers: Phosphate rock, phosphoric acid, Super phosphate and Triple Super phosphate, MAP, DAP. Potassium Fertilizers: Potassium chloride and Potassium sulphate.

TEXTBOOKS:

1.   N.Shreve, "Chemical Process Industries", 5^th Edn., McGraw Hill, New York, 1984.

2.   Austine G.T. – Shreeves Chemicals Process Industries – 5^th Ed. McGraw Hill 1984.

3.      Dryden C.E., M. Gopala Rao – Outlines of Chemical Technology – 3^rd Ed. Affiliated EastWest Press, New Delhi.

4.      Pandey G.N. – Chemical Technology Volume – I – Lion Press, Kanpur.

 REFERENCES:

1.      R.Gopal Rao and M.Sittig,"Dryden's Outlines of Chemical Technology", 3^rd Edn.,Affiliated East-West Publishers,1997.

2.       S.D. Shukla and G.N. Pandey, "Text book of Chemical Technology", Vol. I, 1977.

Environmental Protection & Pollution Control. (CH-255)

Unit I
Introduction: Interaction of man and environment, overall picture of environmental pollution, environmental air and water quality criteria, standards and acts, effects of pollution, gaseous liquid and solid wastes and their disposal, noise pollution and its control.

Unit II
Air Pollution: Types of pollutants - natural and man made, dispersion of pollutant in the atmosphere, Gaussian dispersion model meteorological factors, stability and inversion of atmosphere, plume behavior, control of air pollution from stationary and mobile sources, classification, selection and introduction of equipments like cyclones, electrostatic precipitators, bag filters, wet scrubbers, settling chambers, etc. Methods of measuring and sampling of gaseous and particulate pollutants in ambient air and industrial waste gases, measurement of smoke density and visibility.

Unit III
Water Pollution: Waste liquid characteristics - physical, chemical composition, biochemical oxygen demand (BOD), pathogenic bacteria and chemical toxicity, types of pollutants in liquid wastes of chemical industries, methods for the treatment of liquid wastes to control pollution, classification viz. physical, chemical and biological methods, selection of equipment like hydrocyclone, settling tanks, filters, ion exchange etc, Methods of sampling, preservation of samples and analysis.

Unit IV
Solid Waste Disposal: Characterization of solid wastes, problems of collection and handling, various processing techniques used in solid waste management such as compaction incineration, composting landfills and biological processing solid waste as resource material

 Unit V.                                                                                                                             NOISE POLLUTION AND ODOUR CONTROL: Sources of noise pollution - noise control criteria, noise exposure index. Control of noise pollution. Odour and its control.

TEXTBOOKS:

1.   M. N. Rao and H. V .N. Rao, "Air pollution", Tata McGraw Hill, New Delhi.

2.   C. S .Rao , "Environment Pollution Control and Environmental Engg.", Tata McGraw  Hill, New Delhi.

5.      Metcalf & Eddy, “Wastewater Engineering Treatment and Reuse” Tata McGraw Hill Edition.

6.      Peavy and Row, “Environmental Engineering”

7.      Buckingham, “Hazardous waste”

REFERENCE:

1.   A.C. Stern," Air Pollution - Engineering Control of Air Pollution", Vol IV, 3rd Edn., 1977.

2.   J. O .M. Bockris, "Environmental Chemistry", 1977.

Environmental Engineering Lab (CH-291)

List of Experiments:

1.     To determine the dissolved oxygen content of the given sample by Winkler method. 

2.     To determine the biochemical oxygen demand of the given wastewater sample. 

3.     To determine the chemical oxygen demand of the given wastewater sample. 

4.     To study the BOD kinetics of the given wastewater sample and to determine the kinetic constant. 

5.     To determine the fluoride content in the given water sample. 

6.     To determine the total suspended solids & dissolved solid in the water sample.

7.     To determine bulk density of the soil sample. 

8.     To determine water holding capacity of the soil sample. 

9.     Determination of sulphate content in wastewater. 

10. Estimation of optimum alum dose for coagulation. 

11. Estimation of Ammonical Nitrogen of wastewater sample. 

12. To Study the Water/Waste Water Analyzing kit. 

13. To Study the atomic absorption spectrophotometer.

                                  Chemical Technology Lab (CH-292)

1.      To determine the viscosity of a viscous liquid by falling sphere method.

2.      Determination of saponification value of oil sample

3.      Application of pH meter to find acidity and alkalinity of a solution.

4.      To Study the Colorimeter.

5.      To Study the Ion-Analyzer. 

6.      To study the hydrolysis of cane sugar solution in the presence of an acid by Fehling’s solution method and find out the reaction constant.

7.      To Study the adsorption of benzoic acid on animal charcoal and room temperature and to determine the Freundlich constants k,n.

8.      Determination of the strength of unknown hydrochloric acid by titrating it against caustic soda  by conducto-metric method.

9.      To determine the % composition of a given binary liquid solution by polarimeter.

10.  To determine the solubility of a sparingly soluble salt in water by conductance measurement.

11.  Determination of pH of mixture of CH₃COOH and CH₃COONa and the dissociation constant of the acid.

12.  Preparation of laundry soap and to determine its yield.

13.  To study the Gas Chromatograph.  

Semester – V

INDUSTRIAL Project MANAGEMENT (HUM 301)

UNIT–I

Fundamentals of Management – I:

Management: Evolution, development, characteristics, principles, philosophy, Nature and function, (MBO), (MBE) their importance characteristics and applications.

UNIT–II

Fundamentals of Management – II:

Organizational Behaviour, Human behaviour, group dynamics. Leadership theories, styles and modern philosophies, motivation approaches and theories, communication, barriers and breakdowns, management information system, use of Computer in Management.

UNIT–III

Introduction to Personnel Management:

Employees, Personnel Management practices, methods, recruitment, selection, interviews, group discussions, training, placement and employees development, wages and incentives, labour welfare, conflict, Negotiations, best practices.

UNIT–IV

Introduction to Marketing and Sales Management:

Marketing concept, principles, functions, market survey and research, concepts of sales and distribution, channels of distribution, salesmanship, sales promotions, methods of advertising, copy right, sales management practices.

UNIT–V

Introduction to Financial Management: 

Nature and scope of Financial Management, goals of financial management, Sources of finance, Permanent long term, Short term Sources, Interest rates, annuity cost of capital, capital structure, decisions, Break-even Analysis, Financial Planning.

Suggested Text books and references:

1. Management Stonier & Freeman

2. Principle of Marketing Philip Kotler

3. Industrial Management K.K. Ahuja

4. Financial Management S.K. Banerjee 

Chemical Reaction Engineering – I (CH-301) 

Unit-I        Classification of reaction, Defintion of reaction rate, Variables affecting the rate, concept of reaction equilibria, order of reaction and its determination, theoretical study of reaction rates, collision and activated complex theory, Mechanism of reaction series, Parallel and consecutive reaction autocatalytic reactions, chain reaction polymerization reaction. Interpretation of kinetic data, Integral and differential method of analysis, variable volume reactions, total pressure method of kinetic analysis.

Unit-II       Classification of Reactors: Concept of ideality, Development of design equations for batch, semi batch, tubular and stirred tank reactor, Design of Isothermal and non-isothermal batch, CSTR, PFR, reactors. Combination of reactors, Reactors with recycle, yield and selectivity in multiple reactions.

Unit-III     Multiple Reactions in Batch, continuous stirred tank and plug flow reactors uniqueness of steady state in continuous stirred tank reactor, optimum temperature progression, thermal characteristics of reactors.

Unit-IV      Non-ideal reaction, RTD dispersion model, Tank and series model, recycle model, segregated flow in mixed models, evaluation of RTD characteristics.

Suggested Readings:

1.     O. Levenspiel – Chemical Reaction Engineering – 2^nd Ed. Willey Eastern, Singapore. 

2.     Houghen Watson & Ragatz – Chemical Process Principles Part – III – (Kinetics & Catalysis) 2^nd Ed. Asian Publishing House Bombay. 

3.     Fogler, H.S. – Elements of Chemical Reaction Engineering – 2^nd Ed. Prentice Hall of India Pvt. Ltd. New Delhi – 1999. 

4.     J.M. Smith – Chemical Engineering Kinetics – 3^rd Ed. McGraw Hill. 

5.     K.G. Denbigh & K.G. Turner – Chemical Reaction Theory an Introduction – 2^nd Ed. United Press and ELBS 1972. 

6.     G. Copper & GVJ Jeffery’s – Chemical Kinetics and Reactor Engineering – Prentice Hall 1972

7.      

Mass Transfer – I  (CH-302)

Unit-I        Diffusion Phenomenon: 

                  Molecular and eddy diffusion in gases, liquids and solids, interface mass transfer, Mass transfer theories: film theory, Penetration theory and surface renewal theory.

Unit-II       Concepts of Mass Transfer Coefficient: 

                  Individual and film coefficients, overall mass transfer co-efficient and their inter relationships. Continuous contact and differential contact, mass transfer concepts of NTU and HTU, their inter relationship for dilute phase and concentrated phase contact absorption, extraction and distillation.

Unit-III     Humidification and Drying: 

                  Humidification: General Theory, psychometric chart, fundamental concepts in humidification & dehumidification, wet bulb temperature, adiabatic saturation temperature, measurement of humidification calculation of humidification operation, cooling towers and related equipments. Drying : Equilibrium mechanism theory of drying, drying rate curve. Batch and continuous drying for tray driers, Drum dryers, spray and tunnel dryers.

Unit-IV      Leaching and Extraction:

                  Leaching: solid liquid equilibrium, Equipment, principles of leaching, concurrent and counter current systems and calculation of number of stage required.

Unit-V       Liquid-Liquid extraction:

                  Liquid equilibrium & Ponchon – Savarit method, packed & spray column, conjugate curve and tie line data, plait point, ternary liquid-liquid extraction, operation and design of extraction towers analytical & graphical solution of single and multistage operation in extraction, Co-current, counter current and parallel current system.

Suggested Readings:

1.      McCabe, W.L. Smith J.M. – Unit Operation in Chemical Engg. – 5^th edition Tat McGraw Hill-Hogakucha, Tokyo, New Delhi.

2.      Coulson J.M. Richardson J.F. – Chemical Engg. – Vil-2 Edition-2, Butserworth Heinmann, Oxford, New Delhi.

3.      Treybal R.E. – Mass Transfer Operation- 3^rd edition, McGraw Hill ok Co. New York.

Heat Transfer -I (CH-303) 

Unit I 

Introduction to heat transfer and general concepts of heat transfer. by conduction, convection and radiation. Mechanism of Heat Transfer, Heat Transfer flux and resistance. heat rate equations.

Unit II

Conduction: Basic concepts of conduction in solids liquids and gases, steady state temperature fields and one dimensional conduction without heat generation e.g. through plane walls, Cylindrical and spherical surfaces, composite layers etc.

Unit III 

Theory of insulation, critical radius calculations, types of insulation material, Study state head conduction through slab, cylinder and sphere, critical and optimum insulation thickness. Extended surfaces, fines and their practical applications.

Unit IV 

Convection: Fundamentals of convection, basic concepts and definitions. Natural and forced convection, hydrodynamic and thermal boundary layers, laminar and turbulent heat transfer inside and outside tubes. Heat transfer in boundary layer and in films, co/counter/cross current contacting for heat transfer, individual and overall heat transfer coefficient, fouling factor.

Unit V

Heat Transfer with Phase change: Condensation of pure and mixed vapours, filmwise and dropwise condensation, loading in condensers and basic calculation on condensers, heat transfer in boiling liquids, boiling heat transfer coefficients.

Suggested Readings:

1.     Donald Q. Kern – Process Heat Transfer – Tata McGraw Hill. 

2.     Alan J. Chapman – Heat Transfer – IV Ed. – Collier Mcmillan. 

3.     Heat Transfer by Y.V.C. Rao. 

4.     J.P. Hallman 

5.     Vinay K. Dutta – PHI (Heat Transfer).

PROCESS DYNAMICS & CONTROL (CH 304) 

Unit-I First Order Systems:

Linear open loop systems - First order and Linearised first order systems - Response to various disturbances.

Unit-II Higher Order Systems:

First order in series - Higher order systems - Response to various disturbances.

Unit-III  Block Diagram:

Controls - Block Diagram - closed loop transfer function - Transient response - Simple alarm Modes of control and controller characteristics.

Unit-IV Stability Analysis:

Stability - Routh analysis - Frequency response - Control system design - Controller tuning.

Unit-V Special Controls: 

Cascade - feed forward and ratio control - dead time compensation - Internal Model Control - Control valves - Process identification.

TEXT BOOKS: 

1.    D. P. Coughnowr & Koppel, "Process Systems Analysis and Control", McGraw Hill, New York, 1991. 

2.    C. A. Smith and A. B. Corripio, "Principles and Practice of Automatic Process Control", Wiley, New York, 1989. 

3.    Stephnopalis PHI 

REFERENCES:

1.    P. Harriot, "Process Control" , Tata McGraw Hill, New Delhi, 1984. 

2.    D.P. Eckman, "Industrial Instrumentation", Wiley Eastern Ltd., New York 1990. 

BIOCHEMICAL ENGINEERING (CH 305) 

Unit-I Introduction To Bioscience:

Types of Microorganisms: Structure and function of microbial cells. Fundamentals of microbial growth , batch and continuous culture. Isolation and purification of Enzymes from cells. Assay of Enzymes.

Unit-II Functioning Of Cells And Fundamental Molecular Biology: 

Metabolism and bio-energetics, Photosynthesis, carbon metabolism, EMP pathway, tricarbocyclic cycle and electron transport chain, aerobic and anaerobic metabolic pathways. Synthesis and regulation of biomolecules, fundamentals of microbial genetics, role of RNA and DNA .

Unit-III Enzyme Technology And Kinetics:

Applied Enzyme catalysis , Applications of enzymes in industry and medicine. Immobilization of enzymes. Kinetics of enzyme catalytic reactions involving isolated enzymes. Reversible inhibition.

Unit-IV Reactions Catalysed By Enzymes, Reactors, Analysis:

Reactor Design and Analysis for soluble enzyme systems. Cofactor regeneration . Membrane reactor . Effect of mass transfer in immobilised enzyme particle systems. Reactors for immobilised enzyme systems.

Unit-V Bio Reactors , Effect Of Transport Processes:

Introduction to Bioreactor design: Continuously Stirred aerated tank bioractors. Mixing power correlation .Determination of volumetric mass transfer rate of oxygen from air bubbles and effect of mechanical mixing and aeration on oxygen transfer rate, heat transfer and power consumption. Multiphase bioreactors and their applications. Downstream processing and product recovery in bioprocesses .

TEXT BOOKS: 

1.    J. E. Bailey and D. F. Ollis. " Biochemical Engineering Fundamentals", 2^nd Edn., McGraw Hill, New York , 1986.

2.    Trevan, Boffey, Goulding and Stanbury," Biotechnology", Tata McGraw Hill Publishing Co., New Delhi, 1987. 

REFERENCE: 

M. L. Shuler and F. Kargi, “Bio Process Engineering: Basic concepts”, 2^nd Edn., Prentice Hall of India, New Delhi, 2002. 

Heat Transfer Lab (CH-341)

List of experiments:

1.     To determine the thermal conductivity of metal rod. 

2.     To determine the equivalent thermal conductivity of composite wall. 

3.     To determine heat transfer coefficient in force convection. 

4.     To determine heat transfer coefficient in Natural convection. 

5.     To determine heat transfer coefficient with the help of Steafan Boltzman Apparatus. 

6.     To calculate emmissivity of the test plate by emissivity measurement apparatus. 

7.     To determine heat transfer coefficient in double pipe heat exchanger. 

8.     To study the heat transfer characteristics of a shell and tube heat exchanger (heating/cooling) of water. 

9.     To determine heat transfer coefficient in parallel and counter flow heat exchanger. 

10. To measure the rate of evaporation using an open pan evaporator. 

11. To measure the rate of condensation of pure water vapour and to determine the heat transfer coefficient. 

12. Demonstrate the film-wise drop-wise condensation and determination of the heat transfer coefficient. 

13. To study the single effect evaporator and find out the transfer corfficient.

MECHANICAL OPERATIONS Lab (CH-342)

1. Sphericity factor on friction losses. 

2. Agitated vessel 

3. Settling studies 

4. Drag studies 

5. Filtration (constant rate)

6. Filtration (constant pressure) 

7. Screening 

8. Elutriation Clarification, cyclone separator    

9. Jaw crusher

10.Ballmill 

11. Particle size distribution 

12. Storage of Solids

13. Cyclone studies, Multiple cyclone, mixer – screw type ribbon type   

 Semester – VI  

Computational Methods in Chemical Engineering (CH-351)

Unit-I        Treatment of Engineering data – Graphical representation. Empirical equations, Interpolation, Newton’s formula, Lagrange’s Interpolation formula, extrapolation, Integration, graphical Integration, Graphical Construction of Integral curves, Numerical Integration.

Unit-II       Interpretation of Engineering Data – Significant figure, Classification of Measurements, Propagation of Errors, Variation and Distribution of Random Errors, Properties of Variance and Distribution of Random Errors, Properties of Variance, Confidence limits for small samples.

Unit-III     Ordinary Differential Equations – Formulation, Application of Law of Conservation of Mass – Mixing in flow process. Classification of ordinary Differential Equations and its applications to common Chemical Engineering problems.

Unit-IV      Numerical Solutions of Ordinary Differential Equations-Linear Second- order Equations with variable coefficients, Numerical solution by Runge – Kutta Method. Its application to higher – order equations.

Unit-V       Formulation of partial Differential Equations. Finite difference, linear finite difference equations, nonlinear difference equations. Optimization, types of methods, its application relating to chemical processes.

Suggested Readings:

1.     Mickley, H.S. Sherwood, T.S. Read – Applied Mathematics in Chemical Engineering – Tata McGraw Hill pub.

2.  Jenson & Jeffrey’s – Mathematical Methods in Chemical Engineering.

3. S.K. Gupta - Mathematical Methods in Chemical Engineering.

Mass Transfer – II (CH 352)

Unit-I       Fundamentals of Mass Transfer : Analogies in transfer processes Determination of mass transfer co-efficient; two phase flow in packed beds, co-current and counter current processes loading flooding, column internals: types of trays/plates and packing, point and plate efficiency.

Unit-II       Distillation: Vapour liquid Equilibria, Me-Cave Thefe Method Boiling point diagram, Relative volatility, flash and differential distillation for two component mixture, steam distillation, azeotropic distillation, extractive distillation.

Unit-III     Continuous and Differential contact Distillation:

                  Rectification, reflux ratio, calculation of numbers of plates by NTU, optimum reflux ratio, open steam, multiple feed and multiple product calculations, Enthalpy concentration diagram, Panchon-Savarit method for calculation of number of theoretical plates. Approximate equation; Fensky and undeinrood equation for minimum numbers of plate calculation, Polarison Oililand method for actual numbers of plate calculation, Batch distillation.

Unit-IV      Absorption: Absorption and Extraction in continous contact columns, co-current and cross current contacting fluids, calculations of NTU and HTU, concept of HETP.

Unit-V       Adsorption: Adsorption theories, types of adsorbent; activated carbon, silica and molecular sieves. Batch and column adsorption. Break through curves, Liquid percolation and gas adsorption, BDST models for adsorption calculation.

Suggested Readings:

1.     Treybal R.E. – Mass Transfer operation – 3^rd Ed. McGraw Hill. 

2.     McCabe W.L. Smith J.M.- Unit operation in Chemical Engineering – 3^rd Ed. Tat McGraw Hill. 

3.     Coulson J.M. Richardson J.F. – Chemical Engineering – Vol 2 2^nd Ed. 

4.     Sherwood, T.K. Pigford R.L. and Wllke, C.R. – Mass Transfer- 3^rd Ed. McGraw Hill.

Process Equipment Design –I (CH-353)

Unit-I        Mechanics of materials : Stress – Strain relationships of elastic materials subjected to tensile, compressive and shear forces, Elastic and plastic deformation, Bending moment and bending stress, Torsion, creep and fatigue, theories of column; Thermal stress, membrane stresses in stresses of revolutions, stress concentrations, Theories of failures.

Unit-II       General design considerations; Design codes; Design pressure; Design temperature; Design stress; materials; welded joint efficiencies; corrosion allowances; Design loads, liquid storage tank codes, classification, design of shell, bottom plates, self supported, and column supported roofs, wind girder, nozzles and other accessories.

Unit-III     Unfired pressure vessel: Pressure vessel codes, classification of pressure vessels, Design of cylindrical and spherical shell under internal and external pressures; Selection and design of flat plate, torisperical, ellipsoidal, and conical clousures, compensations of openings.

                  High pressure Vessels: Stress analysis of thick walled cylindrical shell, Design of monobloc and multiplayer vessels.

Unit-IV      Tall vertical & horizontal vessels: Pressure dead weight, wind, earthquake and eccentric loads and induced stresses; combined stresses, Shell design of skirt supported vessels. Vessel supports; Design of skirt, lug, and saddle supports.

Unit-V       Bolted Flanges: Types of Flanges, and selection, Gaskets, Design of non-standard flanges, specifications of standard flanges. Fabrication of equipment major fabrication steps; welding, non destructive tests of welded joints, inspection and testing, vessel lining, materials used in fabrication of some selected chemical industries.

Suggested Readings:

1.     Brownell, N.E. and Young, H.E. – Process Equipment Design – John Wiley (1959) 

2.     Bhattacharya, B.C. – Introduction of Chemical Equipment Design – CBS Publishers, New Delhi. 

3.     I.S. : 2825-1969- Code for Unfired Pressure Vessels. 

4.     I.S.: 803-1962, Code For Practice For Design, Fabrication and Erection of Vertical And Mild Steel Cylindrical Welded oil storage Tanks. 

5.     Joshi, M.V. – Process Equipment Design. 

6.     Steel tables. 

7.     Data files as supplied by university. 

8.     Applied Process deign in Chemical and Petrochemical Plants, E.E. Ludwig – Gulf Publishing Co. 1964, Vol – I. 

9.      

Chemical Process Technology – II (CH 354) 

Unit I.  NATURAL PRODUCTS PROCESSING:

Production of pulp, paper and rayon. Manufacture of sugar, starch and starch derivatives. Gasification of coal and chemicals from coal.

Unit II. INDUSTRIAL MICROBIAL PROCESSES AND EDIBLE OILS:

Fermentation processes for the production of ethyl alcohol, citric acid and antibiotics. Refining of edible oils and fats, fatty acids. Soaps and detergents.

Unit III. PETROLEUM REFINING AND PETROCHEMICAL PRECURSORS: 

Petroleum refining to produce naphtha, fuel hydrocarbons and lubricants. Processes for the production of petrochemicalprecursors: ethylene,propylene, butadiene, acetylene, synthetic gas, benzene, toluene and xylene. ( Cracking, Catalytic reforming and separation of products)

Unit IV. POLYMER BASED INDUSTRIES AND THEIR CHARACTERISTICS:

Plastics: Production of thermoplastic and thermosetting resins such as polyethylene, polypropylene, phenolic resins and epoxy resins; Polymers and their applications in engineering practice.

Unit V. FIBRE FORMING AND ELASTOMERIC POLYMERS: 

Synthetic fibres: polyamides, polyesters and acrylics from monomers. Processes for the production of natural and synthetic rubbers.

TEXTBOOKS:

1.   G.T. Austin, " Shreve's Chemical Process Industries", 5^th Edn., Mcgraw Hill Book Co., NewYork, 1984.

2.   R. Gopal Rao and M. Sittig, " Dryden's Outline of Chemical Technology",3^rd Edn., Affiliated East-West Publishers, 1990. 

REFERENCE:

1. S.D.ShukIa and G.N. Pandey, "Text book of Chemical Technology", Vol. I, 1977.

Heat Transfer – II (CH 355) 

Unit I

Introduction to unsteady state heat transfer. Dimensional analysis, determination of individual and overall heat transfer coefficients and their temperature dependence, heat transfer in molten metals.

Unit II

Radiation
Basic laws of heat transfer by radiation, black body and gray body concepts, view factors Krichoffs law Solar radiations, Combined Heat Transfer Coefficient by convection and radiation. Radiative heat transfer concept of shape factor, methods of determination of shape factor, radiation exchange in enclosure with black surfaces.

Unit III

Evaporation
Elementary principles, types of evaporators, Single and Multiple effect evaporators and their calculation, thermocompression. design and operation of forward – backward and mixed feed operations, effect of boiling point elevation and hydrostatic head vapour recompressing design of condensers.

Unit IV

Boilers, condensers

Heat transfer under phase change conditions, boiling and condensation of pure components, heat flux temperature diagram for boiling and condensation under vertical and horizontal surfaces, nucleate & pool boiling, effect of surface condition on condensation, correlation for heat transfer under condensation.

Unit V 

Heat Transfer Equipments
Classification, principles and design criteria, types of exchangers viz. Double pipe, shell and tube, plate type,Finned tube, extended surface, cooling towers etc, Furnaces and their classification and
application. Simple calculations on them. General design of shell and tube exchangers, condensers

TEXTBOOKS:

1.                  Holman J.P. “Heat Transfer”, McGraw-Hill,

2.                  Kern, D.Q. “ Process Heat Transfer” McGraw Hill 

3.                  Coulson, J.M. and Richardson, JE., “Chemical Engineering” Pergamon Press. 

4.                  Geankoplis, C.J. “Transport Processes and Unit Operation”, Prentice-Hall. 

5.                  Welty, J.R. Wicks, C.W. Wilson, R.E. and Rorrer, G., “Fundamentals of Monmentum Heat and Mass Transfer” John Wiley & Sons. 

Reaction Engg. Lab. (CH 391) 

List of Experiments:

1.     To determine velocity rate constant of hydrolysis of ethyl acetate by sodium hydroxide. 

2.     To study the rate constant of hydrolysis of an ester-catalyzed by acid. 

3.     To study a consecutive reaction system (hydraulic model) 

4.     To study a parallel reaction system (hydraulic model) 

5.     To study a homogeneous reaction in a semi-batch reactor under isothermal conditions.

6.     Study of non- catalytic homogeneous saponification reaction in CSTR. 

7.     To study a non-catalytic homogeneous reaction in a plug flow reactor. 

8.     To study the residence time distribution behavior of a back mix reactor. 

9.     To study the RTD behavior of a tubular reactor. 

10. To study the RTD behavior of a packed bed reactor.

Mass Transfer Lab. (CH 392)

List of Experiments:

1.     To Study the flooding and loading of packed columns using different types of packing. 

2.     To study different types of plates and packing. 

3.     To prepare the vapor-liquid equilibrium and Boiling point diagram for a binary liquid mixture. 

4.     Determination of relative volatility of a given system of acetic acid water. 

5.     To verify Rayleigh equation for differential distillation of binary system. 

6.     To carry out the steam distillation. 

7.     To study batch distillation. 

8.     To study continuous distillation. 

9.     Studies on packed tower distillation unit. 

10. Studies on the sieve plate distillation uint. 

11. Studies on bubble cap distillation column. 

12. To study the absorption of a gas in a packed column and calculation of NTU and HTU. 

13. To perform batch adsorption and verify Freundlich law and Langmir isotherm.

Minor Project & Seminar (CH 393)

The Project work will involve experimental work, modeling and simulation.

Semester – VII

Transport Phenomenon (CH 401) 

Unit-I        Similarity in momentum, heat and mass-transport – Newton’s laws of viscosity, Fouriers laws of coduction and Fick’s laws of diffusion, Flux-transport property relationships, Estimation of transport properties measurement and correlations, velocity distribution in Laminar flow of falling film. Flow over an inclined plane, a circular tube an annulus and between two parallel plates.

Unit-II       Shell balance approach for developing equations of change for momentum, heat and mass transport, Equations of change and their approximations for transport in one dimension.

Unit-III     Transport equations in turbulent flow and equations for turbulent fluxes. Velocity, temperature and concentration profile for laminar and turbulent flow conditions. Temperature and concentration profiles for conductive and convective transport in solids and fluids.

Unit-IV      Macroscopic momentum and heat balance equations, Kinetic energy calculation. Constant area and variable area flow problems. Flow through bends. Time determination for emptying of vessels.

Suggested Reading

1.     Bird R.B., Stewart W.E. and Lightfoot EW. – Transport Phenomena- & Toppan 1960. 

2.     Brodkey Rs and Hershey – “Transport Phenomena A Unified Approach”  - McGraw Hill Book Co.

Process Equipment Design – II (CH 402)

Unit-I        Scale up criteria and scale up of process equipment. Process design calculations for heat exchange equipment shell and tube heat exchangers general description, heat transfer coefficients and pressure drop by Kerm’s Bells methods rating on existing unit.

Unit-II       Design of a new system having one or more units in series single effect evaporation, multiple effect evaporator with boiling point elevation.

Unit-III     Process design calculations for mass exchange equipment plate and packed column for distillation and adsorption including column diameter and height.

Unit-IV      Detailed process and mechanical design, flash drum, Kettle reboiler, condenser, cooling tower & rotary drier.

Suggested Readings:

1.     Perry, Robert H., Green Don W 7^th Ed- Perry’s Chemical Engineering Handbook-McGraw Hill New Delhi. 

2.     E.E. Ludwig – Applied Process Design in Chemical Petrochemical Plants – Gulf Publishing Co. 1964 Vol. – 2. 

3.     B.D. Smith – Design of Equilibrium Stages. 

4.     Coulson J.M. Richardson J.F. – Chemical Engineering Vol-6^th Ed. Pergaman Process.

Chemical Reaction Engineering – II (CH 403)  

Unit-I        Heterogeneous processes : Catalysis and adsorption; Classification of catalysts, Preparation of catalysts. Promoters and Inhibitors, General mechanism of catalytic reactions surface area and pore size distribution Rate equation of fluid solid catalytic reactions, Hougen-Watson & law models, Procurement and analysis of kinetic data, kinetics of catalyst deactivation.

Unit-II       External transport processes and their effects on heterogeneous reactions yield and selectivity Reaction and diffusion in porous catalysts, isothermal and non-isothermal effectiveness factors, Effect of intraphase transport on yield, selectivity and poisoning, Global reaction rate.

Unit-III     Design of catalytic reactors, Iso thermal & adiabatic fixed bed reactor staged adiabatic reactors, Non-Iso thermal non-adiabatic fixed bed reactors, Fluidized bed reactors, Slurry reactors, Trickle bed reactors.

Unit-IV      Models for fluid-solid non-catalytic reactions, controlling mechanisms, Diffusion through gas film controls.

                  Diffusion through ash layer controls, Chemical reaction controls, fluidized bed reactors with and without elutriation.

Unit-V       Gas-liquid reactions and liquid-liquid reaction, Rate equation based on film theory, Reaction design for instantaneous reactions ad slow reactions, Aerobic Fermentation, Application to Design Tools for Fast Reactions.

Suggested Readings:

1.     J.M. Smith-Chemical Engineering Kinetics – 3^rd McGraw Hill 

2.     O. Levenspiel – Chemical Reaction Engineering – 2^nd Ed. Wiley Eastern, Singapore. 

3.     Fogler, H.S. : Elements of Chemical Reaction Engineering 2^nd Ed. Prentice Hall of India Pvt. Ltd. New Delhi – 1997.  

4.     K.G. Denbig & K.G. Turner – Chemical Theory – An Introduction to Re-Actors – 2^nd Ed. United Press & ELBS 1972 

5.     G. Cooper & G.V.J. Jefferys Chemical Kinetics and Reactor Engineering Prentice Hall 1972. 

6.     Hougen, Watson & Ragatz, Chemical Process Principles Part 3 (Kinetics & Cataysis) 2^nd Ed.

7.      

Bio-Process Technology (CH-411)

Unit-I        Introduction to Bio-Chemical Engineering:

                  Aspects of microbiology, cell theory structure of microbial cells, classification of microorganism, Essential chemicals of life lipids, Sugars and Polysaccharides, RNA and DNA, Amino acids and proteins.

Unit-II       Metabolism and Energetic:

                  Assimilatory and dissimilatory process, metabolic mechanism of the cells. Biochemical Kinetics: Simple enzyme reactions in heterogeneous systems.

Unit-III     Growth cycle, phases for Batch cultivation, mathematical modeling of batch growth, products synthesis Kinetics, overall kinetics and thermal death kinetics of cells and spores.

Unit-IV      Unit Operations in Biochemical Process:

                  Agitation and aeration, gas liquid mass transfer, Determination of oxygen transfer rates, Determination of Kga and KLa scaling of mass transfer equipment. Heat balance and ‘heat transfer correlation for biochemical systems, sterilization, filtration and drying.

Unit-V       Design and Analysis of Bio-Reactors

                  Classification and characterization of different bioreactors. Batch and continuous reactors, tubular, CSTR and tower reactors. Aerobic and anaerobic fermentation – process, design and operation of typical aerobic and anaerobic fermentation processes, Manufacture of microbial products e.g. antibiotics alcohol/wine etc. Use of immobilized enzyme and whole cells for industrial processes.

List of Experiments:

1.     To carry out isolation and identification of microorganism from a soil sample. 

2.     To examine and study the effectiveness of various techniques used for the preservation of microorganisms. 

3.     To study the kinetics of ethanol fermentation. 

4.     To determine the kinetic constants 1.1 max and km for the growth of microorganisms. 

5.     To identify bacterial species using Gram staining tests. 

6.     To determine the reducing sugar in the given fermentation medium. 

7.     To determine the protein in the given fermentation medium.

8.     To determine the total sugar content in the given fermentation medium. 

9.     To study the kinetics of methane fermentation. 

10. To study the kinetics of an enzyme catalyzed reaction. 

11. To study the activity of enzymes in free and immobilized States. 

12. To study the activity of whole cell enzymes in free and immobilized States.

Suggested Readings:

1.     Baily, J.E. and Ollis D.F. – Biochemical Engineering Fundamentals – II Ed. McGraw Hill (1986). 

2.     Coulson and Richardson – Chemical Engineering – Ed. III

SURFACE COATING TECHNOLOGY (CH 412) 

Unit I

History and development of paint industry, paint its definition, function and

classification.

Unit II

Raw material for industry, drying oils, bodies oils natural and synthetic resins, pigments

and extenders.

Unit III

Auxiliaries like driers, plasticizers, softeners, dispersing and flatting agents varnishes and

lacquers,

Unit IV

formulation and manufacturing of paints, machinery used in paint manufactures, methods

of application,

Unit V

Applications of industrial and architectural finishes. Common defects in paint and

varnishes. 

Oil Technology (CH 413)

Unit I

General survey of oils and oil based industries sources of oils and fats, their classification, General properties and utilization, composition of glycosides.

Unit II

Non-glyceride components of oils & fats, Fatty acids & waxes, Methods of introduction of oil fats, extraction solvents and extraction rendering.

Unit III

Refining and hydrogenation of oils, vanspati, margarine, Shorteming.

Unit IV

Soaps raw materials and methods of manufactures, introduction to synthetic detergents

Unit V

Fat splitting, fractionation of fatty acids and recovery of glycerin, Essential oils and

cosmetics. 

Energy Engg (CH 414) 

Unit 1

Energy Scenario

Commercial & Non commercial energy, primary energy resources, commercial energy

production, final energy consumption, energy need of growing economy, long term

energy scenario, energy pricing, energy sector reform, energy & environment, energy

conservation and its importance, re- structuring of the energy supply sector, energy

strategy for future, energy conservation act.

Unit II

Energy Management & Energy Planing

Definition & significance, energy strategy, energy policy & energy planning, two sides of

energy management, sectors of supply side energy management, objective of energy

management, hierarchical levels of supply side energy management, trade off b/w energy

management, energy strategies & energy planning, energy & economy, essential

imperatives & steps in supply side energy planning, energy planning flow for supply side,

essential data for supply side energy planing, infrastructure planning, transportation of

energy, per capita energy consumption, imperatives & steps in user side energy planning,

energy management & control system for demand side, seven principal of energy

management, energy policy of a supply organization & demand side organization,

organization for energy management, training & human resource development,

motivation.

Unit III

Energy Audit & Energy Monitoring, Targeting and Conservation

Introduction, need, types & procedure of energy audits, modern techniques and

instruments for energy audit.

Defining monitoring & targeting, element of monitoring & targeting, data & information

analysis, techniques- energy consumption, production & cumulative sum of differences

(CUSUM).

Energy conservation opportunity, electrical & thermodynamic ECOs, ECOs in chemical

process industries, waste management & recycling of discard material and energy.

Unit IV

Advancement In Technologies & Future Energy Alternatives

Recent advancement in energy technology towards 21st century, transport of energy,

ethanol as a fuel.

Fusion – introduction potential, condition for fusion, magnetic confinement fusion

reactor, cold fusion laser induced fusion.

Biomass –introduction, municipal waste, biomass conversion, wood combustion

Geothermal energy – introduction, origin, nature, resources and exploration, environment

impact, low temperature geothermal resources.

Unit V 

Case Studies

Energy conservation in alcohol industry.

Energy conservation in fertilizer industry and pulps & paper industry.

Energy conservation in different units of refinery likes FCCU, HCU & ADU.

Text Books

1. Hinrich & Kleinbach “Energy : its use and the environment” III ed. Harcourt.

2. Boyle “Renewable Energy : Power for a sustainable future” Oxford.

3. Rao S. & Parulckar B.B. ”Energy technology” khhanna publisher

4. Capenart & Turner “ Guide to energy management ” 6 ed. Keinnedu fairmant press. 

Environmental Impact Assessment & Environmental Audit (CH 415) 

Environmental acts - Their need, historical background, national and international acts; Genesis of environmental acts - General procedure followed in changing a bill into an act; implementation of an act using judiciary, executive and legislative powers and their limitations. Main national acts - Environmental protection agency, air act, water act, water and sewerage Board's Factory act, Municipal acts, acts dealing with hazardous and infections wastes. Environmental impact assessment, environmental audit, general procedures followed in preparing reports incorporating EIA ES and EA. Case laws - Principles of case laws, statutory interpretations, site selection, land use planning, town planning act. ISO: 14000 - its need, procedure to be followed to obtain

ISO:14000 certification, implications of ISO. Environmental management plan, environment management cells, rehabilitation and remediation, NGOs and their role. Environmental and occupational health, industrial hygiene, risk assessment disaster management plan, epidemiology.

Assessment of existing effluent treatment plants, trouble shooting, remedial measures. 

Petroleum & Petrochemical Engg. (CH 421)

Unit-I Primary Processing Of Crude Oil: 

Classification of crude oil, Atmospheric distillation, Vacuum distillation of residue-Products and distillation practice.

Unit-II Secondary Processing Of Crude Oil: 

FCCU, Hydro cracking, Visbreaking, Thermal cracking, Coking, Reforming, Alkylation, Polymerisation and Isomerisation process.

Unit-III Treatment Techniques: 

Treatment techniques for removal of objectionable gases, Odours, to improve performance, Storage stability, Extraction of aromatics, Olefins and recovery operations from petroleum products.

Unit-IV            Petrochemicals:

Chemicals from methane and synthetic gas: Ammonia, Methanol and Hydrogen Cyanide, Chemicals from olefins: Ethylene derivatives, Propylene derivatives and Butylenes derivatives, Aromatics, intermediates for synthetic fibres, Plastics and rubber.

Unit-V Environmental And Safety Aspects In Refinery And Petrochemicals: 

Waste water and effluent gases treatment from alkylation units and petrochemical units, safety aspects in the above industries.

TEXT BOOKS: 

1.    W.L. Nelson, “Petroleum Refinery Engineering”, 4^th Edn., McGraw Hill, New York,1985

2.    B. K. Bhaskara Rao, "Modern Petroleum Refining Processes", 2^nd Edn., Oxford and IBH Publishing Company, New Delhi, 1990. 

REFERENCES : 

1.    G. D. Hobson and W. Pohl., " Modern Petroleum Technology", Gulf Publishers, 2^nd Edn., 1990. 

2.     R. A. Meyers, "Hand book of Petroleum Refining Processes”, McGraw Hill, 1^st Edn., 1980.  

Fertiliser Technology (CH 422) 

Introduction: Plant nutrients, different types of fertilizers and their production in India. Nitrogenous Fertilizers: Different feed stocks. Synthesis gas production by steam-naptha reforming and gas purefication. Ammonia synthesis. Urea manufacturing processes. Manufacture of sulphuric acid and ammonium sulphate. Nitric acid and ammonium nitrate manufacture. Phosphatic Fertilizers: Availability and grinding of rock phosphate,

manufacturing processes for single and triple super- phosphate and phosphoric acid. Mixed Fertilizers: Availability and manufacture of muriate of potash. Mixed Fertilizers: Mono and di-ammonium phosphate, urea ammonium phosphates, NPK complex fertilizers, granulation techniques. Engineering Problems: Fertilizers storage and handling. Corrosion problems in fertilizers industries. Fertilizer plant effluent treatment and disposal.  

Text/Reference Books

1. Slack A.V. “Chemistry and Technology of Fertilizers”, Wiley Iinterscience Publishers.

2. Waggaman W.H., “ Phosphoric Acid, Phosphates and Phosphatic Ferilizers”, Hafner Pub.

3. Austin G.T., “Shreve’s Chemical Processes Industires”, 5th Ed. McGraw Hill.

4. Rao M.G. and Sittig M., “ Dryden’s Outlines of Chemical Technology”, Affiliated

5. East West Press, Delhi. 

Industrial Pollution Control (CH 423)

Stream sanitation. Different equations of self-purification, River standards, Effluent standards, Minimal national standards (MINAS). Sources and effects of various pollutants, Disposal of industrial wastes-on land, in creeks and the sea, in inland streams, into impoundments. Importance of planning location of industries and industrial estates, Common effluent treatment plants, their economics and management. Detailed considerations of wastes from industries such as textile (Cotton, wool, rayon, synthetics), sugar, pulp and paper, distilleries, oil refineries, petrochemicals, pharmaceuticals, dairy, food processing, soaps and detergents, mining, iron and steel, pickling, plating, galvanizing, tanning slaughterhouse, fertilizers, pesticides, dyes and dye intermediates, radioactive wastes. Recovery of hyproducts, reuse of wastewaters with or without treatment. 

Pharmaceutical Technology (CH 424)

Unit-I        Practice of the following unit operation in pharmaceutical industries:

                  Heat transfer, evaporation, distillation, dry, mixing size reduction, crystallization, filtration, size separation, conveying, humidification, air conditioning and refrigeration.

Unit-II       Formulation, development of sterile dosage forms. Production facilities, environmental control and personnel in the production of sterile dosage form, compounding, processing, filtration, sealing, sterilization, packing and labeling of sterile dosage forms. Quality control tests like sterility, pyrogen, clarify, safety and leakage testing.

Unit-III     Types of tablets. Manufacturing of tablets by wet granulation, dry granulation and direct compression. Tablet processing problems and defects, tablet standardization: hardness, friability, weights variation, disintegration, dissolution and content uniformity tests.

Unit-IV      Capsules: Hard gelatin capsule, capsule size, formulation and preparation of filled hard gelatin capsules, soft gelatin capsule, soft gel – manufacturing procedures. Quality control of capsule.

Unit-V       Cosmetics and Toiletries: Introduction, factors to be considered in the formulation of facial cosmetics, dentifrice’s, deodorant, antiperspirants, shampoos, hairdressing and hair removers.

Unit-VI      Pharmaceutical packing: Packing components, types of packing containers and closures, materials used for and their pharmaceutical specification, method of evaluation, stability aspects of packaging materials.

Suggested Readings:

1.     Leon Lachman, H.A. Lieberman, J.L.K. – The Theory and Practice of Industrial Pharmacy – Verghese Publishing House, Hind Rajasthan Building Dadar, Mumbai – 40001. 

2.     Ganderton – Unit Process in Pharmacy. 

3.     D. Hershey, Ed – Chemical Engineering in Medicine And Bodogy – Plenum Press, New York. 

4.     Chemical Engineering in Medicine – Chern. Engg. Prpgrer Syrnp Series No. c 66, Vol 62.

Corrosion Engg. (CH 425)

Basic concepts: Definition and importance; Electrochemical nature and forms of corrosion;

Corrosion rate and its determination.

Electrochemical thermodynamics and kinetics: Electrode potentials; Potential-pH (Pourbiax)

diagrams; Reference electrodes and experimental measurements; Faraday’s laws; Electrochemical polarization; Mixed potential theory; Experimental polarization curves; Instrumentation and experimental procedure.

Galvanic and concentration cell corrosion: Basic concepts; Experimental measurements, and determination of rates of galvanic corrosion; Concentration cells.

Corrosion measurement through polarization techniques: Tafel extrapolation plots; Polarization resistance method; Instrumental methods and Errors in measurement of polarization resistance;

Commercial corrosion probes; Other methods of determining polarization curves.

Passivity: Basic concepts of passivity; Properties of passive films; Experimental measurement;

Applications of Potentiostatic Anodic Polarization; Anodic protection.

Pitting and crevice corrosion: Basic concepts; Mechanisms of pitting and crevice corrosion;

Secondary forms of crevice corrosion; Localized pitting.

Metallurgical features and corrosion: Inter-granular corrosion; Weldment corrosion; De-alloying and dezincification.

Environmental induced cracking: Stress corrosion cracking; Corrosion fatigue cracking; Hydrogen induced cracking; Some case studies; Methods of prevention and testing; Erosion, fretting and Wear.

Environmental factors and corrosion: Corrosion in water and Aaqueous Ssolutions; Corrosion in sulphur bearing solutions; Microbiologically induced corrosion; Corrosion in soil; Corrosion of concrete; Corrosion in acidic and alkaline process streams.

Atmospheric and elevated temperature corrosion: Atmospheric corrosion and its prevention;

Oxidation at elevated temperatures; Alloying; Oxidising environments.

Prevention and control of corrosion: Cathodic protection; Coatings and inhibitors; Material selection and design

Books:

1. Fontana, M.G., “Corrosion Engineering”, McGraw-Hill.

2. Jones, D.A., “Principal and Protection of Corrosion”, Prentice-Hall 

Instrumentation and Process Control Lab.(CH-441)  

List of Experiments:

                  Each student should design a complete process plant with mechanical design details of at least three major equipments.

Major Project and Seminar (CH –442) 

The student would be allotted a project in the beginning of the VII semester itself. The

project will be based on the industry where he/she has undergone inplant training in

industry during summer vacations. He/She would be expected to submit a detailed plant

design report later in the (VIII) semester for the project course(CH-492). In this semester

he/she will be assessed for the work that he/she does during the seventh semester under the supervision of a faculty of the department. 

Educational Tour and Training (CH-443)

The students are required to undergo inplant training in some chemical industry for a six

weeks period during their summer vacations following VI semester. He/ she is required to

collect information’s relating to process details and other information’s related to process

material, utilities and their properties to prepare a report to be submitted to the

department. The student would be assessed in the VII semester through a Viva-voce to be

conducted by the teacher incharge training of Chemical Engineering Department.

Semester – VIII

Process Modeling & Simulation. (CH 451)

 Unit-I       The Role of Analysis:

                  Chemical Engineering Problems, basic concepts analysis: The analysis process, A simple example of estimating an order. Source of the model equation: conservation equations, constitutive equation, control volumes, Dimensional analysis, System of units, Dimensional consistency in mathematical descriptions, Dimensional analysis and constitute relationships, Final observations.

Unit-II       Non-reacting Liquid Systems:

                  Introduction, equation of continuity, simple mass balance, application of the model equations, component mass balances. Model behavior : Steady state behavior, Unsteady state behavior, density assumption, Numerical intercal integration methods of ordinary differential equation.

                  Reacting liquid systems: Introduction, basic model equations for a Tank-Type reactor, The reaction rate, The batch reactor, pseudo First-order reactions, Reversible reactions, multiple reactions: consecutive reactions, parallel reactions, complex reactions, constant density assumption, order and stoichiometry.

Unit-III     Treatment of Experimental Data:

                  Introduction, criteria for Best Slope-I, Best Slope-II, Best straight line, Physical property correlations, Fitting a quadratic. Simulation examples of gravity fluid flow, heat and mass transfer, monte-carto simulation.

Unit-IV      Dynamic modeling of simple processes, sequential, simultaneous modular and equation oriented approaches, partitioning and tearing.

Unit-V       Computer programming of various iterative convergence methods such as Newton-Raphson, False position, wegstein, Muller methods.

List of Experiments:

1.     Process dynamics experiments like flow of incompressible fluids at variable flow rate. 

2.     Dyynamics of a tank draining through an orifice in the bottom. Differential equation formulation and verification with the experimental data. 

3.     Mass balance in a tank filling at certain rate and emptying at another rate. Rectangular and wedge-shaped tank and incompressible fluid. 

4.     Modeling a batch reactor-verification of 151 and 2^nd order rate kinetics. 

5.     Counter current double pipe heat exchanger modeling-data analysis by iterative methods. 

6.     Simulation of a distillation column-binary systems, equimolal overflow, constant relative, volatility. 

7.     Input-Output response study in non-ideal flow reactors. 

8.     Simulation of perfectly mixed reactor with heat transfer. Derivation of a mathematical model and solving for study state heat transfer.

Suggested Readings:

1.     Russell T.W.F. – Introduction to Chemical Engineering Analysis – John Wiley & Sons New – York. 

2.     Luyben W.L. – Process Modelling, Simulation and control for Chemical Engineers – II Ed. McGraw Hill Publishing Co. New York – 1990.

Process Engineering & Costing (CH 452)

Unit-I        System and subsystem in process engineering, System analysis, Economic degree of freedom various algorithms, Synthesis of processes, Flow sheeting, Mathematical representation of steady state flow sheet.

Unit-II       Equal time value of money, equivalence comparisons, discrete interest and continuous interest, development of its formula, comparison of alternative investment based on capitalized cost.

Unit-III     Economic Design Criteria Terms involved in profitability analysis, Gross income, depreciation, taxes, net profit, rate of return, venture profit, payout time break even point.

Unit-IV      Time value of money, net present value and venture worth. Capital cost and manufacturing cost estimation methods, Economic analysis and evaluation. Sensitivity & risk analysis, simplifying scale-up cost estimation.